HRID1633215

反应详情

EQUATION

反应方程式

HRID 1633215 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Aminoguanidinium bicarbonate (27.2 g of 98.5%, 0.2 mole) was slurried in 150 ml of water. Sulfuric acid (10.2 g of 96%, 0.1 mole) was added over 1/4 hour with the evolution of carbon dioxide. After post-reacting one hour at room temperature, 125 ml of water were vacuum stripped. On cooling a white precipitate formed which was filtered and dried. Obtained were 11 g of product.

WORKUP

后处理

  1. customAfter post-reacting one hour
  2. customat room temperature
  3. temperatureOn cooling a white precipitate
  4. customformed which
  5. filtrationwas filtered
  6. customdried
  7. customObtained