4-Chlorobenzenesulfonyl chloride → 4-chlorobenzene-1-sulfonohydrazide

HRID 1633229Notes

Reaction equation

HRID 1633229 reaction equation
NC1C(C=[N:11][NH:12][S:13]([C:16]2[CH:21]=[CH:20][C:19]([Cl:22])=[CH:18][CH:17]=2)(=[O:15])=[O:14])=NC(Cl)=C(Cl)N=1.ClC1C=CC(S(Cl)(=O)=O)=CC=1.NN>>[Cl:22][C:19]1[CH:18]=[CH:17][C:16]([S:13]([NH:12][NH2:11])(=[O:14])=[O:15])=[CH:21][CH:20]=1

Participants

4

Reactant 3

HCID 73984-Chlorobenzenesulfonyl chlorideHCID 9321HydrazineHCID 54414708HCID 54414708, compound

Product 1

HCID 2268134-chlorobenzene-1-sulfonohydrazide

Procedure

p-Chlorobenzenesulfonic acid 2-[(3-amino-5,6-dichloropyrazinyl)methylene]hydrazide by the reaction of p-chlorobenzenesulfonyl chloride with hydrazine to form p-chlorobenzenesulfonylhydrazine, followed by the reaction of the latter with 3-amino-5,6-dichloropyrazinaldehyde.

Sources & evidence

ORD record
ord-de4bcb242c4f4c488b433f69d6c95288
Source dataset
uspto-grants-1984_10
Patent number
US04479953

Reaction notes

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