HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12763317, compound → HCID 54415279, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12763317 | HCID 12763317 | — |
| Reactant | 3-amino-1-(6-benzoylamino-9H-purin-9-yl)-1,3-dideoxy-beta-D-ribofuranuronic acid | HCID 53854008 | — |
| Product | HCID 54415279 | HCID 54415279 | 59.2% |
Reaction Steps
1-(6-Benzoylamino-9H-purin-9-yl)-3-[2-(4-nitrobenzyloxycarbonyl)-2-phenylacetylamino]-1,3-dideoxy-β-D-ribofuranuronic acid (315 mg) was prepared by reacting 1-(6-benzoylamino-9H-purin-9-yl)-1,3-dideoxy-3-amino-β-D-ribofuranuronic acid (300 mg) prepared in Example 1 with N-hydroxysuccinimide ester of 2-(4-nitrobenzyloxycarbonyl)-2-phenylacetic acid (386 mg) according to a similar manner to that of Example 5, mp. 168°-175° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04479942 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-e232de3a65994eb69b4e6a2b23c3864a |
| Source note | uspto-grants-1984_10 |