HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzil-di(beta-bromoethyl)ketal → Benzil-di-(beta-1,2,5,6-tetrahydrophthalimidoethyl)ketal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzil-di(beta-bromoethyl)ketal | HCID 2326685 | — |
| Reactant | Sodium 1,2,5,6-tetrahydrophthalimide | HCID 67418806 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Benzil-di-(beta-1,2,5,6-tetrahydrophthalimidoethyl)ketal | HCID 20440919 | 87.6% |
Reaction Steps
Benzil-di-(β-bromoethyl)ketal (13.26 g) and 11.42 g of sodium 1,2,5,6-tetrahydrophthalimide were dissolved in 100 ml of N,N-dimethylformamide, and reacted and worked up in the same way as in Example 4. There was obtained 15.3 g (yield 85.9%) of benzil-di-(β-1,2,5,6-tetrahydrophthalimidoethyl)ketal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04480094 |
| Source dataset | uspto-grants-1984_10 |
| ORD ID | ord-def4ef84b5e34bb5a15020aaf91cf331 |
| Source note | uspto-grants-1984_10 |