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N-3-Bromopropylphthalimide → {2-[(3-Aminopropyl)(3-nitropyridin-2-yl)amino]phenyl}(phenyl)methanone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-3-Bromopropylphthalimide | HCID 21611 | — |
| 反応物 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 反応物 | Sodium hydride | HCID 24758 | — |
| 反応物 | {2-[(3-Nitropyridin-2-yl)amino]phenyl}(phenyl)methanone | HCID 13388384 | — |
| 生成物 | {2-[(3-Aminopropyl)(3-nitropyridin-2-yl)amino]phenyl}(phenyl)methanone | HCID 53831951 | — |
反応手順
[2-[(3-Nitro-2-pyridinyl)amino]phenyl]phenylmethanone is reacted with (a) sodium hydride in solvent followed by N-(3-bromopropyl)phthalimide. The product of (a) is reacted with alcholic hydrazine hydrate and acid to give the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04480100 |
| 出典データセット | uspto-grants-1984_10 |
| ORD ID | ord-41b9eba574c2496c9775dd7d6608bd15 |
| 出典メモ | uspto-grants-1984_10 |