HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isatoic Anhydride → HCID 11435429, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isatoic Anhydride | HCID 8359 | — |
| Reactant | L-Alanine, ethyl ester, hydrochloride (1:1) | HCID 2724356 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 11435429 | HCID 11435429 | 48.5% |
Reaction Steps
Following the method of Example 5 isatoic anhydride (61.3 mmol) was allowed to react with L-alanine ethyl ester HCl (73.6 mmol) in pyridine (200 mL) to give 29.7 mmol of (3S)-3-methyl-3,4-dihydro-1H-1,4-benzodiazepine-2,5-dione as a light, brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06503900B2 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-268490503c344e04b39a7340135cda3b |
| Source note | uspto-grants-2003_01 |