HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl isocyanate → HCID 18677047, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl isocyanate | HCID 76639 | — |
| Reactant | HCID 18677073 | HCID 18677073 | — |
| Product | HCID 18677047 | HCID 18677047 | — |
Reaction Steps
Catalytic hydrogenation of (7-nitro-5-oxo-2,3-dihydro-5H-benzo[f][1,4]oxazepin-4-yl)-acetic acid (Example 15 c) followed by treatment of the resulting amine with benzylisocyanate yielded [7-(3-benzyl-ureido)-5-oxo-2,3-dihydro-5H-benzo[f][1,4]oxazepin-4-yl]-acetic acid: mp. 60-70° C. (dec.); MS (ISP): 370 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06506744B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-1a59e36431744dc5837e3e809fc02434 |
| Source note | uspto-grants-2003_01 |