Methyl 2-(carbonochloridoyl)benzoate → HCID 18677343, compound

HRID 1634133Notes

Reaction equation

HRID 1634133 reaction equation
[Cl:1][C:2]1[C:12]([Cl:13])=[CH:11][C:5](/[CH:6]=[CH:7]/N(C)C)=[C:4]([N+:14]([O-])=O)[CH:3]=1.C[O:18][C:19]([C:21]1[CH:29]=[CH:28][CH:27]=[CH:26][C:22]=1C(Cl)=O)=[O:20]>>[Cl:13][C:12]1[CH:11]=[C:5]2[C:4](=[CH:3][C:2]=1[Cl:1])[NH:14][C:7]([C:22]1[CH:26]=[CH:27][CH:28]=[CH:29][C:21]=1[C:19]([OH:20])=[O:18])=[CH:6]2

Participants

3

Reactant 2

HCID 11159939Methyl 2-(carbonochloridoyl)benzoateHCID 22675057HCID 22675057, compound

Product 1

HCID 18677343HCID 18677343, compound

Procedure

Starting from trans-4,5-dichloro-2-nitro-β-dimethylaminostyrene and 2-(methoxycarbonyl)benzoyl chloride and following successively the procedures of Descriptions 2, 3 and 4 afforded the title compound as a light brown solid which was used without further purification in the next step.

Sources & evidence

ORD record
ord-a3f8f1c94a744bf48243cb60a779db09
Source dataset
uspto-grants-2003_01
Patent number
US06506758B2

Reaction notes

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