HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methylfurfural → HCID 18677563, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methylfurfural | HCID 12097 | — |
| Reactant | O-mesitylenesulfonylhydroxylamine | HCID 11009332 | — |
| Reactant | HCID 18677533 | HCID 18677533 | — |
| Product | HCID 18677563 | HCID 18677563 | 21% |
Reaction Steps
The title compound was prepared in accordance with the general method of example 365 from 2-bromo-N-(2,6-diamino-pyridin-4-ylmethyl)-benzamide, o-mesitylene-sulfonylhydroxylamine, and 5-methyl-2-furaldehyde. The purification was performed with column chromatography on silica eluting with dichloromethane/ethylacetate 1:2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06506772B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-76668e2fb737410a9e2b216666fc1202 |
| Source note | uspto-grants-2003_01 |