HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl isocyanate → HCID 67551045, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | HCID 69843510 | HCID 69843510 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67551045 | HCID 67551045 | 89% |
Reaction Steps
A solution of the product of Example 28 (50 mg, 0.12 mmol) and phenyl isocyanate (17 mg, 0.13 mmol) in DMF (2 mL) was heated at 60° C. for 10 h. The resulting precipitate was filtered, triturated with MeOH/CH2Cl2 (90:10), and dried to provide the title compound (57 mg, 89%) mp>290° C.; MS (ES) 547 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06506769B2 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-5ae5a8ad456c4154b6f82e6b8246eaa9 |
| Source note | uspto-grants-2003_01 |