HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Methyltyramine → HCID 18678923, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Methyltyramine | HCID 4657 | — |
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18678923 | HCID 18678923 | 97.9% |
Reaction Steps
A mixture of methyl acrylate (6.0 g, 69.7 mmol) and p-methoxyphenethyl amine (10.5 g, 69.7 mmol) in anhydrous methanol (88 mL) was refluxed for 3 days and then was concentrated to give methyl 3-[(4-methoxyphenethyl)amino]-propionate (16.2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06506936B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-f5cbe89a42e24d3787d3e6650e705f74 |
| Source note | uspto-grants-2003_01 |