反应详情

A mixture of t-butyl-[4-benzyloxyphenoxy]-diphenylsilane (170 g, 388 mmol) and 10 g of 10% palladium on carbon in ethanol-cyclohexene (2:1, v/v) was heated at reflux for 48 hours. The catalyst was filtered and the solvent was removed in vacuo to provide 134 g of product as an oil.

1. temperaturev/v) was heated
2. temperatureat reflux for 48 hours
3. filtrationThe catalyst was filtered
4. customthe solvent was removed in vacuo