m-Chloroperbenzoic acid → HCID 88088784, compound

Participants

Reaction Steps

4-{[t-butyl(diphenyl)silyl]oxy}-2-chlorobenzaldehyde (11.00 g, 28 mmol) was dissolved in CHCl3 (150 ml). In one portion m-chloroperbenzoic acid (MCPBA) (7.21 g, 41.8 mmol) was added and the solution heated to reflux for 72 h. The solution was diluted with CH2Cl2, washed with sat. NaHSO3, sat. NaHCO3, brine and dried (MgSO4). The solvent was removed to provide 9.42 g of the title compound.

Provenance & Evidence