HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 70000670, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | Tert-butyl (piperidin-4-ylmethyl)carbamate | HCID 723429 | — |
| Reactant | 4-(3-Methyl-2-oxo-1-imidazolidinyl)benzenesulfonyl chloride | HCID 18678416 | — |
| Product | HCID 70000670 | HCID 70000670 | 65% |
Reaction Steps
Prepared according to the procedure used for example 46 (Step A, part 1) from piperidin-4-ylmethyl-carbamic acid t-butyl ester (1.09 g, 5.1 mmol), 4-(3-methyl-2-oxo-imidazolidin-1-yl)-benzenesulfonyl chloride (1.4 g, 5.1 mmol) and 0.89 mL of diisopropylethyl amine to give 1.5 g of the title compound
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06506901B2 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-c055468cd1b64ddea4c7dcca4fb8bf2c |
| Source note | uspto-grants-2003_01 |