3,4,5-Trimethoxybenzeneboronic acid → Ethyl 6-(3,4,5-trimethoxyphenyl)picolinate

HRID 1634884Notes

Reaction equation

HRID 1634884 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5](B(O)O)[CH:6]=[C:7]([O:11][CH3:12])[C:8]=1[O:9][CH3:10].Cl[C:17]1[N:22]=[C:21]([C:23]([O:25][CH2:26][CH3:27])=[O:24])[CH:20]=[CH:19][CH:18]=1>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([C:17]2[N:22]=[C:21]([C:23]([O:25][CH2:26][CH3:27])=[O:24])[CH:20]=[CH:19][CH:18]=2)[CH:6]=[C:7]([O:11][CH3:12])[C:8]=1[O:9][CH3:10]

Participants

3

Reactant 2

HCID 27343903,4,5-Trimethoxybenzeneboronic acidHCID 11063114Ethyl 6-chloropicolinate

Product 1

HCID 18675009Ethyl 6-(3,4,5-trimethoxyphenyl)picolinate

Procedure

3,4,5-Trimethoxyphenylboronic acid (837 mg) and ethyl 6-chloropicolinate (733 mg) were reacted in the same manner as in Preparation Example 1 to obtain the title compound.

Sources & evidence

ORD record
ord-d44ac96aaaa24ea1afc37507aaf67bfe
Source dataset
uspto-grants-2003_01
Patent number
US06509329B1

Reaction notes

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