HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophene-3-boronic acid → Tert-butyl 2-nitro-4-thien-3-ylphenylcarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophene-3-boronic acid | HCID 581760 | — |
| Reactant | Tert-butyl (4-iodo-2-nitrophenyl)carbamate | HCID 23554339 | — |
| Product | Tert-butyl 2-nitro-4-thien-3-ylphenylcarbamate | HCID 66865115 | — |
Reaction Steps
Prepared from (4-iodo-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example A1) and 3-thiopheneboronic acid according to the general procedure B. Obtained as a yellow solid (326 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06509328B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-293469c2ff95448fbfc4cc8c13266b7d |
| Source note | uspto-grants-2003_01 |