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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1635154Generated: October 31, 2026

3-Iodotoluene → (3'-Methyl-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester

https://huagongshe.com/reaction/1635154

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-IodotolueneHCID 12268—
ReactantBis(pinacolato)diboraneHCID 2733548—
ReactantTert-butyl (4-iodo-2-nitrophenyl)carbamateHCID 23554339—
Product(3'-Methyl-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl esterHCID 69592827—

Reaction Steps

Prepared from (4-iodo-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example A1), bis(pinacolato)diboron and 3-iodotoluene according to the general procedure C. Obtained as a yellow solid (524 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06509328B1
Source datasetuspto-grants-2003_01
ORD IDord-3383a4da948d450d8b215bb80c49bd09
Source noteuspto-grants-2003_01