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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1635156Generated: October 26, 2026

1-Chloro-2-iodobenzene → (2'-Chloro-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester

https://huagongshe.com/reaction/1635156

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Chloro-2-iodobenzeneHCID 11993—
ReactantBis(pinacolato)diboraneHCID 2733548—
ReactantTert-butyl (4-iodo-2-nitrophenyl)carbamateHCID 23554339—
Product(2'-Chloro-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl esterHCID 69592813—

Reaction Steps

Prepared from (4-iodo-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example A1), bis(pinacolato)diboron and 1-chloro-2-iodobenzene according to the general procedure C. Obtained as a yellow oil (886 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06509328B1
Source datasetuspto-grants-2003_01
ORD IDord-3222ca9cfd504aaf9b4abac5922d5152
Source noteuspto-grants-2003_01