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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1635157Generated: October 25, 2026

2-Iodotoluene → (2'-Methyl-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester

https://huagongshe.com/reaction/1635157

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-IodotolueneHCID 5128—
ReactantBis(pinacolato)diboraneHCID 2733548—
ReactantTert-butyl (4-iodo-2-nitrophenyl)carbamateHCID 23554339—
Product(2'-Methyl-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl esterHCID 67290097—

Reaction Steps

Prepared from (4-iodo-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example A1), bis(pinacolato)diboron and 2-iodotoluene according to the general procedure C. Obtained as a yellow oil (755 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06509328B1
Source datasetuspto-grants-2003_01
ORD IDord-02f9f814670f4bb492ac3c15bf70aeb9
Source noteuspto-grants-2003_01