HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromopyridine → (2-Nitro-4-pyridin-3-yl-phenyl)-carbamic acid tert.-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromopyridine | HCID 12286 | — |
| Reactant | Bis(pinacolato)diborane | HCID 2733548 | — |
| Reactant | Tert-butyl (4-iodo-2-nitrophenyl)carbamate | HCID 23554339 | — |
| Product | (2-Nitro-4-pyridin-3-yl-phenyl)-carbamic acid tert.-butyl ester | HCID 69592765 | — |
Reaction Steps
Prepared from (4-iodo-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example A1), bis(pinacolato)diboron and 3-bromopyridine according to the general procedure C. Obtained as a yellow solid (587 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06509328B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-ecc6d33d55c146f78bc4237ceb50e93a |
| Source note | uspto-grants-2003_01 |