HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Ethynyltoluene → HCID 69592839, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Ethynyltoluene | HCID 13018 | — |
| Reactant | Tert-butyl (4-iodo-2-nitrophenyl)carbamate | HCID 23554339 | — |
| Product | HCID 69592839 | HCID 69592839 | 89.7% |
Reaction Steps
Prepared from (4-iodo-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example A1) (728 mg, 2.0 mmol) and 4-tolylacetylene (349 mg, 3.0 mmol) according to the general procedure F. Obtained as a yellow solid (632 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06509328B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-d69b08402de74c829750a494d45e13ea |
| Source note | uspto-grants-2003_01 |