HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl (4-(furan-3-yl)-2-nitrophenyl)carbamate → (2-Amino-4-furan-3-yl-phenyl)-carbamic acid tert.-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl (4-(furan-3-yl)-2-nitrophenyl)carbamate | HCID 69592767 | — |
| Catalyst | Nickel | HCID 935 | — |
| Product | (2-Amino-4-furan-3-yl-phenyl)-carbamic acid tert.-butyl ester | HCID 69592861 | — |
Reaction Steps
Prepared from (4-furan-3-yl-2-nitrophenyl)-carbamic acid tert.-butyl ester (Example B6) by catalytic hydrogenation with Raney-Ni according to the general procedure G (method a). Obtained as a light brown solid. (744 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06509328B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-ca6ed3d5cb884179b2474a6b91b9791b |
| Source note | uspto-grants-2003_01 |