HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic acid, 3-cyano-, methyl ester → 3-(3-Cyano-phenyl)-3-oxo-propionic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic acid, 3-cyano-, methyl ester | HCID 83554 | — |
| Reactant | Lithium Tert-butyl Acetate | HCID 86586795 | — |
| Product | 3-(3-Cyano-phenyl)-3-oxo-propionic acid tert-butyl ester | HCID 69592889 | — |
Reaction Steps
Prepared from methyl 3-cyanobenzoate [CAS-No. 13531-48-1] by treatment with lithium tert.-butyl acetate according to general procedure H (method b). Obtained as a light brown oily semisolid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06509328B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-d8c06568b0c441a8b6283dbdec5905a6 |
| Source note | uspto-grants-2003_01 |