HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(2,2-Dimethyl-6-oxo-6H-[1,3]dioxin-4-yl)-benzonitrile → {3-[3-(3-Cyano-phenyl)-3-oxo-propionylamino]-[1,1';4',1''] terphenyl-4-yl}-carbamic acid tert.-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(2,2-Dimethyl-6-oxo-6H-[1,3]dioxin-4-yl)-benzonitrile | HCID 11736337 | — |
| Reactant | HCID 69592771 | HCID 69592771 | — |
| Product | {3-[3-(3-Cyano-phenyl)-3-oxo-propionylamino]-[1,1';4',1''] terphenyl-4-yl}-carbamic acid tert.-butyl ester | HCID 86588016 | 66.7% |
Reaction Steps
Prepared from (3″-amino-[1,1′;4′,1″]terphenyl-4″-yl)-carbamic acid tert.-butyl ester (Example G32) (159mg, 0.44mmol) and 3-(2,2-dimethyl-6-oxo-6H-[1,3]dioxin-4-yl)-benzonitrile (Example J4) (111 mg, 0.49 mmol) according to the general procedure K. Obtained as an off-white solid (156 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06509328B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-bfbbc7e699a940ef97d1278fd3e10892 |
| Source note | uspto-grants-2003_01 |