6-Methyl-2,4-bis-methylsulfanylpyridin-3-ylamine → HCID 70027628, compound

HRID 1635481Notes

Reaction equation

HRID 1635481 reaction equation
[C:1]1([C:7]2[C:8]3[CH:22]=[CH:21][CH:20]=[CH:19][C:9]=3[O:10][CH2:11][C:12]=2[CH:13]=[CH:14][CH2:15][C:16](O)=[O:17])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:23][S:24][C:25]1[C:30]([NH2:31])=[C:29]([S:32][CH3:33])[CH:28]=[C:27]([CH3:34])[N:26]=1>>[CH3:23][S:24][C:25]1[C:30]([NH:31][C:16](=[O:17])[CH2:15][CH:14]=[CH:13][C:12]2[CH2:11][O:10][C:9]3[CH:19]=[CH:20][CH:21]=[CH:22][C:8]=3[C:7]=2[C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)=[C:29]([S:32][CH3:33])[CH:28]=[C:27]([CH3:34])[N:26]=1

Participants

3

Reactant 2

HCID 99903926-Methyl-2,4-bis-methylsulfanylpyridin-3-ylamineHCID 54093295HCID 54093295, compound

Product 1

HCID 70027628HCID 70027628, compound

Procedure

N-[2,4-Dimethylthio-6-methyl-3-pyridyl]-4-(4-phenyl-2H-3-benzo[b]pyranyl)but-3-enamide is prepared under the conditions of Example 1 from 4-(4-phenyl-2H-3-benzo[b]pyranyl)but-3-en-1-oic acid and 2,4-dimethylthio-6-methyl-3-pyridylamine.

Sources & evidence

ORD record
ord-c847f435c10246799d85956a1bceac2d
Source dataset
uspto-grants-2003_01
Patent number
US06509362B2

Reaction notes

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