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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1635546Generated: October 28, 2026

HCID 66758637, compound → HCID 86585735, compound

https://huagongshe.com/reaction/1635546

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 66758637HCID 66758637—
CatalystHCID 178418406HCID 178418406—
SolventDichloromethaneHCID 6344—
SolventEthyl AcetateHCID 8857—
ProductHCID 86585735HCID 8658573593.4%

Reaction Steps

To a solution of the product of example 274 (1.0 g) in methylene chloride(200 ml) was added manganese(IV) oxide(3.0 g), and the suspension was stirred at ambient temperature for 12 hours. The reaction mixture was diluted with ethyl acetate and filtered through Celite. The solvent was evaporated under reduced pressure to give the titled compound(930 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06509346B2
Source datasetuspto-grants-2003_01
ORD IDord-822a3ff7b746448d969c9887a0535429
Source noteuspto-grants-2003_01