HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Chloro-4-fluoro-5(3-trifluoromethyltriazolyl)phenyl]methyl sulfide → HCID 131723750, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Chloro-4-fluoro-5(3-trifluoromethyltriazolyl)phenyl]methyl sulfide | HCID 22567417 | — |
| Reactant | 2-Chloro-4-fluoro-5(3-trifluoromethyltriazolyl)thiophenol | HCID 68659326 | — |
| Product | HCID 131723750 | HCID 131723750 | 85.7% |
Reaction Steps
2.2 g (7.1 mmol) of [2-chloro-4-fluoro-5(3-trifluoromethyltriazolyl)phenyl]methyl sulfide was converted to 2-chloro-4-fluoro-5(3-trifluoromethyltriazolyl)thiophenol in the same manner as in Reference Example 1 and then to 1.8 g of 1,1′-thiodi-[2-chloro-4-fluoro-5-(3-trifluoromethyltriazolyl)benzene (yield 85.7%) in the same manner as in Reference Example 5 (1), which was used in Example 2 (4) as the starting material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06509354B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-0c8adac52cde454e8b52a398f3a40fb7 |
| Source note | uspto-grants-2003_01 |