HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 178519454, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 10132459 | HCID 10132459 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178519454 | HCID 178519454 | — |
Reaction Conditions
| Temperature | 100 °C |
|---|
Reaction Steps
To a solution of 3-chloro-4-(5H,11H-pyrrolo[2,1-c][1,4]-benzodiazepine-10-carbonyl)-benzonitrile (0.348 g) in dimethylformamide (2 ml) was added sodium azide (0.078 g) and ammonium chloride (0.065 g). The mixture was heated to 100° C. for 18 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06511974B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-4a6ca3e63fda46f3b184b2bf9df491ca |
| Source note | uspto-grants-2003_01 |