HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 5-bromovalerate → ethyl 5-(9H-carbazol-2-yloxy)-pentanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 5-bromovalerate | HCID 84580 | — |
| Reactant | 2-Hydroxycarbazole | HCID 93551 | — |
| Product | ethyl 5-(9H-carbazol-2-yloxy)-pentanoate | HCID 18674670 | 34.3% |
Reaction Steps
In a manner analogous to that of example 6(a), ethyl 5-bromo-pentanoate (685 mg, 3.28 mmol) was reacted with 2-hydroxycarbazole (600 mg, 3.28 mmol) to give ethyl 5-(9H-carbazol-2-yloxy)-pentanoate (350 mg, 34%) as a colorless solid. MS (MH+)310.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06512123B2 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-1760b067aa36470aa2f10a2f320e07d0 |
| Source note | uspto-grants-2003_01 |