HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86588285, compound → HCID 86588284, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86588285 | HCID 86588285 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86588284 | HCID 86588284 | 16% |
Reaction Steps
Using General Procedure B with 1.14 9 (2.09 mmol) (2 E,4 E)-(R)-1-[6-[(R)-2-Benzyloxycarbonyl-pyrrolidin-1-yl]-2,5-dimethyl-6-oxo-hexa-2,4-dienoyl]-pyrrolidine-2-carboxylic acid benzyl ester and with dioxane as solvent afforded 127 mg (16%) of the title compound as a white solid. MS mie (%): 365 (M+H+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06512001B1 |
| Source dataset | uspto-grants-2003_01 |
| ORD ID | ord-24939ad361f645ae8fa11e8141c615b1 |
| Source note | uspto-grants-2003_01 |