HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(tert-butoxycarbonyl)glycine → N-[2-(N-tert-Butyloxycarbonyl-glycyl-glycyl)-amino-2-deoxy-beta-D-glucopyranosyl]-N-tetradecyl-oleamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(tert-butoxycarbonyl)glycine | HCID 78288 | — |
| Reactant | N-(2-glycyl-amino-2-deoxy-beta-glucopyranosyl)-N-tetradecyl-oleamide | HCID 131721258 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | N-[2-(N-tert-Butyloxycarbonyl-glycyl-glycyl)-amino-2-deoxy-beta-D-glucopyranosyl]-N-tetradecyl-oleamide | HCID 131721721 | 68% |
Reaction Steps
from N-(2-glycyl-amino-2-deoxy-β-D-glucopyranosyl)-N-tetradecyl-oleamide and N-tert-butyloxycarbonyl-glycine. Yield 68%. [α]D =+14.5° (c=0.92, tetrahydrofuran).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06034055 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-4c889121991b4fb8ad23a2e3988c8543 |
| Source note | uspto-grants-2000_03 |