Potassium Hydroxide → HCID 54127341, compound

HRID 1636297Notes

Reaction equation

HRID 1636297 reaction equation
[CH2:1]([O:8][CH2:9][CH:10]([CH2:16][O:17][Si](C(C)(C)C)(C)C)[O:11][CH2:12][C:13]([OH:15])=[O:14])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[OH-].[K+]>CO.O>[CH2:1]([O:8][CH2:9][CH:10]([CH2:16][OH:17])[O:11][CH2:12][C:13]([OH:15])=[O:14])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

5

Reactant 2

HCID 14797Potassium HydroxideHCID 19350803HCID 19350803, compound

Product 1

HCID 54127341HCID 54127341, compound

Reagents, catalysts & solvents 2

HCID 887MethanolSolventHCID 962WaterSolvent

Procedure

1-O-Benzyl-3-t-butyldimethylsilyl-2-O-carboxymethylglycerol (5 g) was dissolved in methanol (50 ml), and a solution of 85% potassium hydroxide (7 g) in water (50 ml) was added thereto. The mixture was stirred at room temperature for 60 hours to complete the reaction.

Workup

  1. customthe reaction

Sources & evidence

ORD record
ord-40883fc41b9148ac916a41b45fb3005b
Source dataset
uspto-grants-2000_03
Patent number
US06034087

Reaction notes

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