HCID 19351298, compound → HCID 178458326, compound

HRID 1636334Notes

Reaction equation

HRID 1636334 reaction equation
[CH3:1][C:2]1[C:6](=[CH:7][NH2:8])[C:5](=[O:9])[N:4]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[N:3]=1.[CH2:16]([O:19][C:20]1[CH:33]=[CH:32][CH:31]=[CH:30][C:21]=1NOC(=O)C(F)(F)F)[CH2:17][CH3:18]>C(O)C>[CH3:1][C:2]1[C:6](=[CH:7][NH:8][C:21]2[CH:30]=[CH:31][CH:32]=[CH:33][C:20]=2[O:19][CH2:16][CH2:17][CH3:18])[C:5](=[O:9])[N:4]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[N:3]=1

Participants

4

Reactant 2

HCID 19351298HCID 19351298, compoundHCID 178433860HCID 178433860, compound

Product 1

HCID 178458326HCID 178458326, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

3-methyl-4arninomethylene-1-phenyl-4,5-dihydro-pyrazol-5-one (2 g) and 2-propoxyanilino-trifluoroacetic acid salt (1.6 g) are refluxed 1.5 hours in ethanol.

Sources & evidence

ORD record
ord-0f49dad84a3e4ab199a2a9b6711e5605
Source dataset
uspto-grants-2000_03
Patent number
US06034099

Reaction notes

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