HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → HCID 19351329, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 2-(4-aminophenyl)-2,4-dihydro-5-methyl-3H-pyrazol-3-one | HCID 80815 | — |
| Product | HCID 19351329 | HCID 19351329 | — |
Reaction Steps
From the reaction of 5-methyl-2-(4-aminophenyl)-2,4-dihydro-pyrazol-3-one and methansulfonylchloride (reaction per Example 11, where methanesulfonylchloride is used in respective molecular amounts), N-(4-(4,5-dihydro-3-methyl-5-oxo-1H-pyrazol-1-yl)-phenyl)-N-methylsulfonylmethanesulfonamide is obtained. Subsequent reaction with 2-ethyl aniline yields N-(4-(4-(2-Ethylanilinomethylene)-4,5-dihydro-3-methyl-5-oxo-1H-pyrazol-1-yl)-phenyl)-N-methylsulfonylmethansulfonamide, Mp: 268° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06034099 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-c3b57e62fcc646669e2d120ddd54176a |
| Source note | uspto-grants-2000_03 |