HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Hydrazinobenzenesulphonic acid → 3-(4,5-Dihydro-5-oxo-3-propyl-1H-pyrazol-1-yl)-benzenesulfonic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Hydrazinobenzenesulphonic acid | HCID 67312 | — |
| Reactant | 3-Oxooctanoate | HCID 17804644 | — |
| Product | 3-(4,5-Dihydro-5-oxo-3-propyl-1H-pyrazol-1-yl)-benzenesulfonic acid | HCID 19351347 | — |
Reaction Steps
From the reaction of 3-hydrazinobenzenesulfonic acid and ethylbutyrylacetate, 3-(4,5-Dihydro-5-oxo-3-propyl-1H-pyrazol-1-yl)-benzenesulfonic acid is obtained. Subsequent reaction with 2-ethylaniline yields 3-(4-(2-ethylanilinomethylene)-4,5-dihydro-5-oxo-3-propyl-1H-pyrazol-1-y 1)-benzenesulfonic acid, Mp 258.6° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06034099 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-5cb35f17c68c4e1eabb5d9a7d1177d52 |
| Source note | uspto-grants-2000_03 |