3-Bromophenol → HCID 22571591, compound

HRID 1636431Notes

Reaction equation

HRID 1636431 reaction equation
[C:1](Cl)(=[O:6])[CH2:2][CH2:3][CH2:4][CH3:5].[Br:8][C:9]1[CH:10]=[C:11]([OH:15])[CH:12]=[CH:13][CH:14]=1>N1C=CC=CC=1>[C:1]([O:15][C:11]1[CH:12]=[CH:13][CH:14]=[C:9]([Br:8])[CH:10]=1)(=[O:6])[CH2:2][CH2:3][CH2:4][CH3:5]

Participants

4

Reactant 2

HCID 115633-BromophenolHCID 61186Valeryl chloride

Product 1

HCID 22571591HCID 22571591, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

Pentanoyl chloride (12.7 g) was added dropwise to 3-bromophenol (9.0 g) in pyridine (50 ml), and the reaction mixture was stirred at room temperature for 1 hour. Work-up as described in Example 12 gave 3-bromophenyl pentanoate.

Sources & evidence

ORD record
ord-65282750c2be433d81b513c1cb79d9b0
Source dataset
uspto-grants-2000_03
Patent number
US06034121

Reaction notes

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