HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Aminophenyl)-6-methylbenzothiazole → HCID 391871, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Aminophenyl)-6-methylbenzothiazole | HCID 7087 | — |
| Reactant | Iodine chloride | HCID 24640 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 391871 | HCID 391871 | 66.7% |
Reaction Steps
2-(4'-Aminophenyl)-6-methylbenzothiazole (0.6 g, 2.5 mmol) was treated with iodine monochloride (0.5 g, 3.02 mmol) in acetic acid according to the above-described general procedure for iodination. Crude product was purified by flash chromatography on silica gel, using ethyl acetate-hexane (1:3) as eluent, to give brown small crystals (0.61 g, 66.7%), m.p. 176.2-177.9° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06034246 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-442f96b0a9c44ac48f43768ccb110f5c |
| Source note | uspto-grants-2000_03 |