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HRID1636569

反应详情

EQUATION

反应方程式

HRID 1636569 的结构方程式

REACTANTS

反应物

4
结构：O=C([O-])[O-].[Na+].[Na+]
HCID10340

Carbonic acid sodium salt (1:2)

CNa2O3

结构：O=S(=O)(O)Cl
HCID24638

Chlorosulfuric acid

HClO3S

结构：NS(=O)(=O)[O-]
HCID177700

Sulfamate ion

H2NO3S-

结构：Cc1cc(-c2nc3ccccc3s2)ccc1N
HCID384525

4-(1,3-benzothiazol-2-yl)-2-methylaniline

C14H12N2S

PRODUCTS

生成物

1
结构：Cc1cc(NS(=O)(=O)[O-])ccc1-c1nc2ccccc2s1.[Na+]
HCID23717893

未命名化合物

收率 82%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccn1
溶剂HCID7975

2-Methylpyridine

C6H7N

PROCEDURE

实验过程

2-(4'-amino-3'-methylphenyl)benzothiazole was treated with chlorsulphonic acid in 2-picoline and sodium carbonate according to the above-described general procedure for preparation of sulphamate salts. A yellow powder was obtained in 82% yield, m.p. 169.5° C. (dec).

WORKUP

后处理

  1. customA yellow powder was obtained in 82% yield, m.p. 169.5° C. (dec)