Imidazole → HCID 19349392, compound

HRID 1636804Notes

Reaction equation

HRID 1636804 reaction equation
[NH:1]1[CH:5]=[CH:4][N:3]=[CH:2]1.Cl[CH:7]([C:9]1[CH:10]=[C:11]([C:20]([CH3:24])([CH3:23])[C:21]#[N:22])[CH:12]=[C:13]([C:15]([CH3:19])([CH3:18])[C:16]#[N:17])[CH:14]=1)[CH3:8]>>[N:1]1([CH:7]([C:9]2[CH:14]=[C:13]([C:15]([CH3:18])([CH3:19])[C:16]#[N:17])[CH:12]=[C:11]([C:20]([CH3:24])([CH3:23])[C:21]#[N:22])[CH:10]=2)[CH3:8])[CH:5]=[CH:4][N:3]=[CH:2]1

Participants

3

Reactant 2

HCID 795ImidazoleHCID 19349417HCID 19349417, compound

Product 1

HCID 19349392HCID 19349392, compound

Procedure

The process described in Example 8 was repeated, using imidazole in place of 1,2,4-triazole, and 2,2'-[5-(1-chloroethyl)-1,3-phenylene]di(2-methylpropiononitrile), (obtained as described in the second part of Example 7), as the starting materials, to give 2,2'-[5-(1-[imidazol-1-yl]ethyl)-1,3-phenylene]di(2-methylpropiononitrile), mp. 77°-80°.

Workup

  1. custom(obtained

Sources & evidence

ORD record
ord-d1d832d913394589b3d83d565a1ce525
Source dataset
uspto-grants-2000_03
Patent number
USRE036617

Reaction notes

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