HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propenoic acid, 3-(3-nitrophenyl)- → 3-(3-Aminophenyl)propionic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propenoic acid, 3-(3-nitrophenyl)- | HCID 68390 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-(3-Aminophenyl)propionic acid | HCID 2735406 | — |
Reaction Steps
3-Nitrocinnamic acid (50 g) was suspended in ethanol (600 cm3) and reduced in the presence of palladium catalyst until no further hydrogen uptake was observed. After filtering the solvent was evaporated under reduced pressure to give the pure product in quantitative yield as a brown oil which slowly crystallised.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06037309 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-7a02d25af6284ef9a228ef45c3dcff95 |
| Source note | uspto-grants-2000_03 |