2-(9H-carbazol-2-yloxy)ethylamine → HCID 18615263, compound

HRID 1636949Notes

Reaction equation

HRID 1636949 reaction equation
Br[CH2:2][C:3]([C:5]1[CH:10]=[C:9]([NH:11][S:12]([CH3:15])(=[O:14])=[O:13])[CH:8]=[C:7]([O:16][CH2:17][C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[CH:6]=1)=[O:4].[CH:24]1[C:36]2[NH:35][C:34]3[C:29](=[CH:30][CH:31]=[CH:32][CH:33]=3)[C:28]=2[CH:27]=[CH:26][C:25]=1[O:37][CH2:38][CH2:39][NH2:40]>CO.C(Cl)(Cl)Cl>[CH:24]1[C:36]2[NH:35][C:34]3[C:29](=[CH:30][CH:31]=[CH:32][CH:33]=3)[C:28]=2[CH:27]=[CH:26][C:25]=1[O:37][CH2:38][CH2:39][NH:40][CH2:2][CH:3]([C:5]1[CH:6]=[C:7]([O:16][CH2:17][C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[CH:8]=[C:9]([NH:11][S:12]([CH3:15])(=[O:14])=[O:13])[CH:10]=1)[OH:4]

Participants

4

Reactant 2

HCID 110854932-(9H-carbazol-2-yloxy)ethylamineHCID 18615151HCID 18615151, compound

Product 1

HCID 18615263HCID 18615263, compound

Reagents, catalysts & solvents 1

HCID 21584188Chloroform methanolSolvent

Procedure

170 mg of Intermediate 62 and 95 mg of Intermediate 2. Rf=0.28 (methanol/chloroform of 1/9).

Sources & evidence

ORD record
ord-154a63d17b944e44930c9106bd738256
Source dataset
uspto-grants-2000_03
Patent number
US06037362

Reaction notes

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