HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 2,3-Pentanedione, 2-(O-methyloxime)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2,3-Pentanedione, 2-oxime | HCID 6797453 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 2,3-Pentanedione, 2-(O-methyloxime) | HCID 54196011 | — |
Reaction Steps
49.7 g (0.35 mol) of methyl iodide are added dropwise at room temperature to a solution of 40.2 g (0.55 mol) of pentane-2,3-dione 2-oxime and 52.0 g (0.38 mol) of potassium carbonate in 400 ml of acetone, and stirring is continued for 12 hours at this temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06037378 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-2f9349ac3f064c46942de8fef4f99321 |
| Source note | uspto-grants-2000_03 |