Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Xanthene | HCID 7107 | — |
| Reactant | N-Hydroxyphthalimide | HCID 10665 | — |
| Solvent | Benzonitrile | HCID 7505 | — |
| Product | Xanthone | HCID 7020 | 99% |
Reaction Steps
A mixture of 2 mmole of xanthene, 10 mole % of N-hydroxyphthalimide relative to xanthene, and 5 ml of benzonitrile was stirred for 20 hours at 100° C. under an oxygen atmosphere. The products in the reaction mixture were analyzed by gas chromatography, and, as a result, 9-oxoxanthene (yield not less than 99%) was formed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06037477 |
|---|
| Source dataset | uspto-grants-2000_03 |
|---|
| ORD ID | ord-03dc0090973a486b8d6b2d8fc9795127 |
|---|
| Source note | uspto-grants-2000_03 |
|---|
