HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 961283, compound → HCID 15338901, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 961283 | HCID 961283 | — |
| Reactant | O-(Benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate | HCID 2733207 | — |
| Reactant | N~5~-(tert-Butoxycarbonyl)-N~2~-{[(9H-fluoren-9-yl)methoxy]carbonyl}-D-ornithine | HCID 13996154 | — |
| Product | HCID 15338901 | HCID 15338901 | — |
Reaction Steps
Prepared analogously to Example 33b) from (R)-N5 -(tert.-butoxy-carbonyl)-N2 -(9-fluorenylmethoxycarbonyl)-ornithine and N-methyl-4-(phenylmethoxy)benzenemethanamine in the presence of TBTU in a quantitative yield. Colourless, highly viscous oil, which was used in the following step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06040289 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-75514df933144c8fb751448c4c3521a5 |
| Source note | uspto-grants-2000_03 |