HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-t-Butyl-5-carbamoylaniline → N-(2-t-Butyl-5-carbamoylphenyl)-3-(2,4-dimethoxy-5-methoxycarbonylphenyl)octanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-t-Butyl-5-carbamoylaniline | HCID 19348606 | — |
| Reactant | HCID 19348732 | HCID 19348732 | — |
| Solvent | Ethyl ether methylene chloride | HCID 21881112 | — |
| Product | N-(2-t-Butyl-5-carbamoylphenyl)-3-(2,4-dimethoxy-5-methoxycarbonylphenyl)octanamide | HCID 19348499 | — |
Reaction Steps
Following a similar procedure to that described in Example 44, but using 3-(2,4-dimethoxy-5-methoxycarbonylphenyl)octanoic acid (prepared as described in Preparation 37) and 2-t-butyl-5-carbamoylaniline (prepared as described in Preparation 38), the title compound was obtained as crystals, melting at 101-103° C. (from methylene chloride-diethyl ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06040339 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-fa1bffbb758b4d2ca0ed9c8d8caed67f |
| Source note | uspto-grants-2000_03 |