HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylacetamide → N-[2-t-Butyl-5-(2,2-dimethylpropanoyl)aminocarbonylphenyl]-3-(2,4-dimethoxyphenyl)octanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylacetamide | HCID 12957 | — |
| Reactant | HCID 19348635 | HCID 19348635 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | N-[2-t-Butyl-5-(2,2-dimethylpropanoyl)aminocarbonylphenyl]-3-(2,4-dimethoxyphenyl)octanamide | HCID 19348506 | — |
Reaction Steps
Following a similar procedure to that described in Example 139, but using N-(2-t-butyl-5-carboxyphenyl)-3-(2,4-dimethoxyphenyl)octanamide (prepared as described in Preparation 7) and 2,2-dimethylpropanamide, the title compound was obtained as crystals, melting at 170-172° C. (from ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06040339 |
| Source dataset | uspto-grants-2000_03 |
| ORD ID | ord-8e229cc88ce148f7b546a9d4facfe7d0 |
| Source note | uspto-grants-2000_03 |