3-(2,4-Dimethoxyphenyl)heptanoic acid → HCID 19348738, compound

HRID 1637522Notes

Reaction equation

HRID 1637522 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[C:7]([O:9][CH3:10])[CH:6]=[CH:5][C:4]=1[CH:11]([CH2:16][CH2:17][CH2:18][CH3:19])[CH2:12][C:13]([OH:15])=[O:14].[CH2:20]([Mg]Br)[CH2:21]CCCC>>[CH3:1][O:2][C:3]1[CH:8]=[C:7]([O:9][CH3:10])[CH:6]=[CH:5][C:4]=1[CH:11]([CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21])[CH2:12][C:13]([OH:15])=[O:14]

Participants

3

Reactant 2

HCID 193485383-(2,4-Dimethoxyphenyl)heptanoic acidHCID 178444609HCID 178444609, compound

Product 1

HCID 19348738HCID 19348738, compound

Procedure

Following a similar procedure to that described in Preparation 42a, but using hexylmagnesium bromide instead of butylmagnesium bromide, the title compound was obtained as an oily substance.

Sources & evidence

ORD record
ord-a76a74eb8aa547d6b60bdd6e3c775585
Source dataset
uspto-grants-2000_03
Patent number
US06040339

Reaction notes

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