2-Aminomethyl-1-ethylpyrrolidine → HCID 54476347, compound

HRID 1637594Notes

Reaction equation

HRID 1637594 reaction equation
[CH2:1]([O:6][C:7]1[CH:8]=[C:9]([CH:13]=[CH:14][C:15]=1[O:16][CH2:17][CH:18]=[C:19]([CH3:21])[CH3:20])[C:10]([OH:12])=O)[CH:2]=[C:3]([CH3:5])[CH3:4].[NH2:22][CH2:23][CH:24]1[CH2:28][CH2:27][CH2:26][N:25]1[CH2:29][CH3:30]>>[CH2:29]([N:25]1[CH2:26][CH2:27][CH2:28][CH:24]1[CH2:23][NH:22][C:10](=[O:12])[C:9]1[CH:13]=[CH:14][C:15]([O:16][CH2:17][CH:18]=[C:19]([CH3:21])[CH3:20])=[C:7]([O:6][CH2:1][CH:2]=[C:3]([CH3:4])[CH3:5])[CH:8]=1)[CH3:30]

Participants

3

Reactant 2

HCID 1172952-Aminomethyl-1-ethylpyrrolidineHCID 18799484HCID 18799484, compound

Product 1

HCID 54476347HCID 54476347, compoundYield 55%

Procedure

In a manner identical to Example 15, 3,4-diprenyloxybenzoic acid(1.45 g) was subjected to a condensation reaction with 2-aminomethyl-1-ethylpyrrolidine (0.7 ml), thereby yielding 1.09 g(55%) of the aimed compound. m.p. 80.0-81.5° C.

Sources & evidence

ORD record
ord-9985cd91c2e847b083b245b49937ecfa
Source dataset
uspto-grants-2000_03
Patent number
US06043243

Reaction notes

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