2-Aminomethyl-1-ethylpyrrolidine → HCID 88236303, compound

HRID 1637601Notes

Reaction equation

HRID 1637601 reaction equation
[CH2:1]([C:11]1[CH:19]=[CH:18][CH:17]=[CH:16][C:12]=1[C:13](O)=[S:14])/[CH:2]=[C:3](/[CH2:5][CH2:6][CH:7]=[C:8]([CH3:10])[CH3:9])\[CH3:4].[NH2:20][CH2:21][CH:22]1[CH2:26][CH2:25][CH2:24][N:23]1[CH2:27][CH3:28]>>[CH2:27]([N:23]1[CH2:24][CH2:25][CH2:26][CH:22]1[CH2:21][NH:20][C:13](=[S:14])[C:12]1[CH:16]=[CH:17][CH:18]=[CH:19][C:11]=1[CH2:1]/[CH:2]=[C:3](/[CH2:5][CH2:6][CH:7]=[C:8]([CH3:10])[CH3:9])\[CH3:4])[CH3:28]

Participants

3

Reactant 2

HCID 1172952-Aminomethyl-1-ethylpyrrolidineHCID 178442767HCID 178442767, compound

Product 1

HCID 88236303HCID 88236303, compoundYield 54%

Procedure

In a manner identical to Example 15, 2-geranylthiobenzoic acid(2.03 g) was subjected to a condensation reaction with 2-aminomethyl-1-ethylpyrrolidine (1.0 ml), thereby yielding 1.52 g(54%) of the aimed compound.

Sources & evidence

ORD record
ord-0cb3e7e98e3845c79fae92670eede495
Source dataset
uspto-grants-2000_03
Patent number
US06043243

Reaction notes

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