2-Aminomethyl-1-ethylpyrrolidine → HCID 54356429, compound

HRID 1637610Notes

Reaction equation

HRID 1637610 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[C:10]([O:14][CH2:15][CH:16]=[C:17]([CH3:19])[CH3:18])[C:11]=1[O:12][CH3:13])[C:6]([OH:8])=O.[NH2:20][CH2:21][CH:22]1[CH2:26][CH2:25][CH2:24][N:23]1[CH2:27][CH3:28]>>[CH2:27]([N:23]1[CH2:24][CH2:25][CH2:26][CH:22]1[CH2:21][NH:20][C:6](=[O:8])[C:5]1[CH:9]=[C:10]([O:14][CH2:15][CH:16]=[C:17]([CH3:19])[CH3:18])[C:11]([O:12][CH3:13])=[C:3]([O:2][CH3:1])[CH:4]=1)[CH3:28]

Participants

3

Reactant 2

HCID 1172952-Aminomethyl-1-ethylpyrrolidineHCID 18799501HCID 18799501, compound

Product 1

HCID 54356429HCID 54356429, compoundYield 157.4%

Procedure

In a manner identical to Example 15, 3,4-dimethoxy-5-prenyloxybenzoic acid (0.80 g) was subjected to a condensation reaction with 2-aminomethyl-1-ethylpyrrolidine (0.39 g), thereby yielding 1.78 g(69%) of the aimed compound.

Sources & evidence

ORD record
ord-5b49203597dd45ea83ac996349d360e8
Source dataset
uspto-grants-2000_03
Patent number
US06043243

Reaction notes

Loading…